This book preparation is an effort made to cover the practicals of physical pharmaceutics to be performed during the B.Pharm curriculum. The practicals cover topics related to physical properties of liquids like surface tension, viscosity, density, pH, stability of suspensions. Special emphasis is given on the procedure of practicals which will be helpful for the teachers and students with greater ease of understanding the concepts of physical pharmaceutics. It was found that very few such books were available having practical matter as compared to the books having theory matter. So this book will be very helpful to academicians as well as the industry in understanding the concepts of physical pharmaceutics.