This book presents select proceedings of the International Conference on Future Learning Aspects of Mechanical Engineering (FLAME 2020). This book, in particular, focuses on characterizing materials using novel techniques. It covers a variety of advanced materials, viz. composites, coatings, nanomaterials, materials for fuel cells, biomaterials among others. The book also discusses advanced characterization techniques like X-ray photoelectron, UV spectroscopy, scanning electron, atomic power, transmission electron and laser confocal scanning fluorescence microscopy, and gel electrophoresis chromatography. This book gives the readers an insight into advanced material processes and characterizations with special emphasis on nanotechnology.